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5137-55-3
Methyl trioctyl ammonium chloride CAS 5137-55-3
  • CAS:

    5137-55-3
  • Molecular Formula:

    C25H54ClN
  • Quality Standard:

    90%
  • Packing:

    180kg/drum
  • Factory Site:

    Anhui, China
  • Mininmum Order:

    1000kg
  • Price inquiry:

    sales@tnjchem.com
  • Manufacturer:

    TNJ Chemical

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  • Product Details
  • Reference COA

Synthesis method of Methyl trioctyl ammonium chloride CAS 5137-55-3

1. Autoclave method

396 g (1 mole) of N235 and 300 ml of ethanol were mixed in the autoclave, and the autoclave was used for ice-acetone cooling. Then pour 2 moles of methyl chloride (pre-frozen and liquefied, collected in an Erlenmeyer flask), immediately close the autoclave, stir and heat to 100, react under a pressure of <10 kg/cm2 for 4 to 5 hours, and cool to room temperature , Release residual methyl chloride. Then the ethanol is removed by vacuum distillation to obtain a brown product weighing about 430 grams (95-100%).

2. Atmospheric pressure method

100 ml (52 g, 0.2 mol) of N235 and isooctanol with a volume ratio of 1.5:1 to N236 were placed in a tubular reactor, and methyl chloride was introduced at a flow rate of 150 ml/min for about 20 minutes. Then heated to 130°C. Methyl chloride was introduced at the flow rate of tiny bubbles, and reacted for 5 to 7 hours. After cooling, the reactant is transferred to a liquid film evaporator, and the product is obtained by vacuum distillation at 120-130°C/3-5mm to evaporate the solvent. The conversion rate is 60-70%.

 

Methyl trioctyl ammonium chloride CAS 5137-55-3 is viscous colorless to pale orange liquid,with the melting point at-20°C boiling point at 240°C, density at 0.884 g/ml at 25 °C(lit.),Fp >230 °F.It is stable. Incompatible with strong oxidizing agents. Hygroscopic.


Specification 

Appearance                        Light yellow to yellow viscous liquid

Active Matter %                  90±2%
Free Amine %                     2%
PH(1% aqueous solution)    4-8

 

Application
Widely used as a fungicide, disinfectant and bactericide in water treatment, swimming pool, livestock, hospital/personal health care

Packing
180kg/drum, 14.4MT/FCL

Storage

Placed in sealed container and kept in a cool and dry place.
Avoid strong vibration, insolation, high temperature, smoke and fire.

Product name

Methyl trioctyl ammonium chloride

B atch No .

20240323

CAS . No .

5137-55-3

Package

180.00kg/drum

M. F.

(C8H17)3CH3NCl

MFG date

Mar. 23 , 2024

N. W.

14 , 400 . 00kg

A nalysis  date

Mar. 23 , 2024

G. W.

15, 600 . 00kg

Expiry date

Mar. 22 , 2025

 

 Items

 Specification

 Testing  Results

 Appearance

 Yellow to yellowish  viscous liquid

 Yellowish  viscous liquid

 Active matter,  %

 90  ±10

 90 . 3

 Free Amine ,  %

 ≤2 . 0

 1 . 1

 pH  ( 1% Aqueous solution)

 4 . 0 ~ 8 . 0

 5.2

Specific gravity,  25   C

 0 . 9 ~ 0 . 93

 0 . 93


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